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科研系列
技术系列
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姓名: |
吴石头 |
性别: |
男 |
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职称: |
高级工程师 |
学历: |
博士 |
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电话: |
010-82998670 |
传真: |
010-62010846 |
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Email: |
shitou.wu[a]mail.iggcas.ac.cn |
邮编: |
100029 |
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地址: |
北京朝阳区北土城西路19号,中科院地质与地球物理研究所 |
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简历: |
* 吴石头,高级工程师,硕士生导师,1987年出生于河北石家庄。长期从事LA-(MC)-ICP-MS分析方法研发及其应用研究。主要研究成果:(1) 研发了磷钇矿、磷灰石、石榴石、褐帘石和独居石等富镥矿物的激光微区Lu-Hf定年方法,极大地拓宽了微区可定年矿物的范围;(2) 通过系统优化和改进质谱仪硬件,使得仪器灵敏度提升5-10倍,基于此,开发了激光微区方解石U-Pb定年技术,将锆石U-Pb定年空间分辨率提升至5-16微米,建立了微区低损耗/低含量元素分析方法; (3) 研制了10件微区元素/同位素标准物质(ARM-1, ARM-2, ARM-3, OJY-1, OH-1, OA-1, TLM, LSJ07, KNW和SK10-3),丰富了现有微区分析标准物质数据库。目前以第一/通讯作者发表论文28篇,授权中国发明专利5项,美国发明专利1项;主持翻译英文著作1部。曾获国家建设高水平大学公派研究生项目(201306410007)。目前担任《地球化学》青年编委(2022-2025),《地球科学》《Journal of Earth Science》两刊青年编委(2023-2025)。 * 教育及工作经历: 2007/09-2011/06,中国地质大学(武汉),应用化学,获工学学士学位 2011/09-2013/06,中国地质大学(武汉),应用化学,获工学硕士学位 2013/10-2017/09,德国哥廷根大学,地球化学,获理学博士学位 2018/03-2020/12,中科院地质与地球物理研究所,工程师 2024/01-2024/03,美国德州理工大学(TTU),访问学者
2021/01-至今,中科院地质与地球物理研究所,高级工程师
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研究方向: |
元素/同位素微区分析标准物质研发; 副矿物U-Th-Pb年代学实验方法开发; 原位微区Lu-Hf定年分析技术及地质应用 月球玄武岩成因
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获奖及荣誉: |
- 中国科学院技术支撑人才(2023)
中国科学院青年创新促进会会员(2022) 2023年所级优秀科技成果奖(排名第1) 2021年所级优秀科技成果奖(排名第14) 2020年所级优秀科技成果奖(排名第3)
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承担科研项目情况: |
- 国家自然科学基金面上基金项目(斜锆石U-Pb和Hf同位素标准物质研制及小束斑(5-20微米)定年技术,批准号:42273034,2023/01-2026/12),主持,在研
- 国家自然科学基金青年基金项目(飞秒激光-三重四级杆ICP-MS准确测定石英和锆石中微量元素钛,批准号:41903024,2020/01-2022/12),主持,结题
- 岩石圈演化国家重点实验室开放课题(激光剥蚀-高灵敏度ICPMS定量分析橄榄石、斜方辉石、单斜辉石中的痕量元素(<50 ng g-1),批准号:SKL-K201805,2018/07-2020/12),主持,结题
- 所级中心短期技术访问项目(LA-ICP-MS元素二维Mapping分析技术,2019),主持,结题
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代表论著: |
Google Scholar Research Gate 第一作者或通讯作者(*)论文 - Ranran Chen, Shitou Wu*, Hao Wang, Martin Senger, André Navin Paul, Paul J. Sylvester, Yueheng Yang, Jinhui Yang, and Fuyuan Wu. 2024. Baddeleyite SK10-3: A natural reference material for microbeam U–Pb geochronology and Hf isotopic analyses. Geostandards and Geoanalytical Research. Accepted.
- Junlong Niu, Shitou Wu*, Yueheng Yang, Hao Wang, Chao Huang, Lei Xu, Liewen Xie. 2024. Robust determination of low Ti contents in zircon using LA–ICP–MS/MS with NH3 reaction gas. Journal of Analytical Atomic Spectrometry, DOI https://doi.org/10.1039/D4JA00304G
- Shitou Wu*, Dingshuai Xue, Yueheng Yang, Hao Wang, Chunlai Li, Fuyuan Wu. 2024. Chemical analysis of Chang’e-5 lunar soil using LA–ICP–MS in highly diluted fused glass discs. Journal of Analytical Atomic Spectrometry, DOI https://doi.org/10.1039/D4JA00329B
- Shitou Wu*, Junlong Niu, Yueheng Yang, Hao Wang, Jinhui Yang, Fuyuan Wu. 2024. First demonstration of in situ Lu–Hf dating using LA-ICP-MS/MS applied to monazite. Journal of Analytical Atomic Spectrometry, DOI: https://doi.org/10.1039/D4JA00258J.
- Shitou Wu*, Yueheng Yang, Hao Wang, Nick M.W. Roberts, Junlong Niu, Yijia Wang, Jinhui Yang, Fuyuan Wu. 2024. In situ LuHf dating of allanite by LA-ICP-MS/MS: Implications for geochronology. Chemical Geology, 122383.
- Jia Meng, Shitou Wu*, Hao Wang*, Yueheng Yang, Chao Huang, Chao Zhang, Wenqiang Yang, Jiarun Tu, Shuiyuan Yang, Qian Ma, Qiang Wang, Lei Xu and Liewen Xie. 2024. The KNW rutile-A natural reference material for microbeam U–Pb age and trace element determinations. Journal of Analytical Atomic Spectrometry, DOI: https://doi.org/10.1039/D4JA00190G.
- Hao Chen, Ming Tang*, Shitou Wu* and Xuanyu Liu. 2024 Determination of ultra-trace rare earth elements in olivine by laser ablation-sector field-inductively coupled plasma-mass spectrometry. Journal of Analytical Atomic Spectrometry. DOI: https://doi.org/10.1039/D4JA00122B .
- 牛俊龙, 吴石头*, 杨岳衡, 张超, 王浩, 龚庆杰. 2024. 石英和锆石Ti温度计在地学中的应用及Ti含量的微区分析技术进展. 岩石学报, 040(01):0323-0337.
- Shitou Wu*, Yueheng Yang, Tianyi Li, Chao Huang, Zhian Bao, Youlian Li, Chaofeng Li, Lei Xu, Hao Wang, Liewen Xie, Jinhui Yang and Fuyuan Wu. 2023 Calcite TLM and LSJ07– two natural low-Sr reference materials for microbeam Sr isotope analysis. Journal of Analytical Atomic Spectrometry. 38, 2528-2537 (封面文章)
- Jiadai Li, Jing Xu*, Shitou Wu*, Nigel J. Cook, Cristiana L. Ciobanu, Sarah Gilbert, Liyuan Wang. 2023 Robust dating of Pb-Zn skarn systems by LA-ICP-MS garnet U-Pb geochronology. Ore Geology Reviews. 159, 105565.
- Shitou Wu, Hao Wang*, Yueheng Yang*, Junlong Niu, Zhongwu Lan, Liangliang Zhang, Chao Huang, Liewen Xie, Lei Xu, Jinhui Yang, Fuyuan Wu, 2023. In situ Lu-Hf geochronology with LA-ICP-MS/MS. Journal of Analytical Atomic Spectrometry. 38, 1285-1300.
- 谢博航, 吴石头*, 杨岳衡, 王浩, 赵子福, 黄超, 谢烈文. 2023. LA-MC-ICP-MS方解石U-Pb定年技术.岩石学报, 039(01): 0236-0248.
- Shitou Wu*, Andreas Audétat, Klaus Peter Jochum, Hao Wang, Jingyuan Chen, Brigitte Stoll, Chao Zhang, Zhian Bao, Shuiyuan Yang, Chaofeng Li, Xuefeng Wang, Chunxue Xu, Lei Xu, Chao Huang, Liewen Xie, Yueheng Yang, Jinhui Yang. 2022. Three Natural Andesitic to Rhyolitic Glasses (OJY-1, OH-1, OA-1) as Reference Materials for In Situ Microanalysis. Geostandards and Geoanalytical Research. 46, 673–700. (GeoReM数据库推荐文章)
- Shitou Wu, Yueheng Yang*, Nick M. W. Roberts, Ming Yang, Hao Wang, Zhongwu Lan, Tianyi Li, Lei Xu, Chao Huang, Liewen Xie, Jinhui Yang and Fuyuan Wu. 2022. In situ calcite U-Pb geochronology by high-sensitivity single-collector LA-SF-ICP-MS. SCIENCE CHINA Earth Sciences, 65 1146-1160.
- Shitou Wu*, Yueheng Yang, Klaus Peter Jochum, Rolf L. Romer, Johannes Glodny, Ivan P. Savov, Samuele Agostini, Jan C.M. De Hoog, Stefan T.M. Peters, Andreas Kronz, Chao Zhang, Zhian Bao, Xiaojun Wang, Youlian Li, Guoqiang Tang, Lianjun Feng, Humin Yu, Zhenxin Li, Zhang Le, Jie Lin, Yuan Zeng, Chunxue Xu, Yaping Wang, Zhu Cui, Li Deng, Jun Xiao, Yanhong Liu, Dingshuai Xue, Zhang Di, Lihui Jia, Hao Wang, Lei Xu, Chao Huang, Liewen Xie, Andreas Pack, Gerhard Woerner, Maoyong He, Chaofeng Li, Honglin Yuan, Fang Huang, Qiuli Li, Jinhui Yang, Xianhua Li, Fuyuan Wu. 2021. Isotopic Compositions (Li-B-Si-O-Mg-Sr-Nd-Hf-Pb) and Fe2+/ΣFe Ratios of Three Synthetic Andesite Glass Reference Materials (ARM-1, ARM-2, ARM-3). Geostandards and Geoanalytical Research, 45, 719–745.(GeoReM数据库推荐文章)
- Shitou Wu*, Ming Yang, Yueheng Yang, Liewen Xie, Chao Huang, Hao Wang and Jinhui Yang. 2020. Improved in situ zircon U–Pb dating at high spatial resolution (5-16 mm) by laser ablation–single collector-sector field-ICP-MS using Jet sample and X skimmer cones. International Journal of Mass Spectrometry, 456, 116394.
- Shitou Wu*, Yueheng Yang, Hao Wang, Chao Huang, Liewen Xie and Jinhui Yang. 2020. Characteristic performance of guard electrode in LA-ICP-MS for multiple element quantification. Atomic Spectroscopy, 41: 154-161.
- Shitou Wu*, Yadong Wu, Yueheng Yang, Hao Wang, Chao Huang, Liewen Xie and Jinhui Yang. 2020. Simultaneous quantification of forsterite content and minor-trace elements in olivine by LA-ICP-MS and geological applications in Emeishan large igneous province. Minerals, 10, 634.
- Shitou Wu*, Gerhard Woerner, Klaus Peter Jochum, Brigitte Stoll, Klaus Simon and Andreas Kronz. 2019. The Preparation and Preliminary Characterization of Three Synthetic Andesite Reference Glass Materials (ARM-1, ARM-2, ARM-3) for in situ Microanalysis. Geostandards and Geoanalytical Research, 43(4): 567-584. (GeoReM数据库推荐文章)
- 吴石头, 许春雪*, 陈宗定, 王亚平, 白金峰. 2019. LA-ICP-MS结合超高压粉末压片技术快速分析碳酸盐岩中的Mg, Ca, Sr, Ba和轻稀土元素. 分析实验室, 38(9): 1089-1094.
- Shitou Wu*, Volker Karius, Burkhard C Schmidt, Klaus Simon and Gerhard Woerner. 2018. Comparison of Ultrafine Powder Pellet and Flux-free Fusion Glass for Bulk Analysis of Granitoids by Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry. Geostandards and Geoanalytical Research, 42(4): 575-591. (GeoReM数据库推荐文章)
- Shitou Wu*, Chao Huang, Liewen Xie, Yueheng Yang and Jihui Yang. 2018. Iolite Based Bulk Normalization as 100% (m/m) Quantification Strategy for Reduction of Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry Transient Signal. Chinese Journal of Analytical Chemistry, 46: 1628-1636.
- Shitou Wu, Yaping Wang* and Chunxue Xu. 2017. Laser ablation-inductively coupled plasma-mass spectrometer: A quantification strategy based on two reference materials and bulk normalization as 100% (wt). Chinese Journal of Analytical Chemistry, 45(7): 965–972
- 吴石头, 许春雪*, Klaus Simon, 肖益林, 王亚平. 2017. 193nm ArF准分子激光系统对LA-ICP-MS分析中不同基体的剥蚀行为和剥蚀速率探究. 岩矿测试, 36(5): 451-459.
- Shitou Wu, Yaping Wang*, Chunxue Xu and Jihai Yuan. 2016. Elemental fractionation studies of 193 nm ArF excimer laser ablation system at high spatial resolution. Chinese Journal of Analytical Chemistry, 44(7): 1035–1041.
- 吴石头, 王亚平*, 詹秀春, Andreas Kronz, Klaus Simon, 许春雪, 田欢. 2016. CGSG系列标准物质元素分馏效应及主量微量元素单元内均匀性探究. 岩矿测试, 35(6), 612-620.
- 吴石头, 王亚平*, 许春雪. 2015. 激光剥蚀电感耦合等离子体质谱元素微区分析标准物质研究进展[J]. 岩矿测试, 34(5), 503-511
- 吴石头, 王亚平*, 孙德忠, 温宏利, 许春雪, 王伟. 2014. 电感耦合等离子体发射光谱法测定稀土矿石中15种稀土元素-四种前处理方法的比较. 岩矿测试, 33(1), 12-19.
代表性合作论文 Zhang, H., Griffiths, M., Chiang, J., Kong, W., Wu, S., Atwood, A., Huang, J., Cheng, H., Ning, Y., Xie, S.,2018. East Asian hydroclimate modulated by the position of the westerlies during Termination I. Science, 362, 580-583. Tian, H.-C.(#), Wang, H. (#), Chen, Y. (#), Yang, W. (*), Zhou, Q., Zhang, C., Lin, H.-L., Huang, C., Wu, S.-T., Jia, L.-H., Xu, L., Zhang, D., Li, X.-G., Chang, R., Yang, Y.-H., Xie, L.-W., Zhang, D.-P., Zhang, G.-L., Yang, S.-H., Wu, F.-Y. 2021 Non-KREEP origin for Chang’E-5 basalts in the Procellarum KREEP Terrane. Nature, 600, 59-63.
英文译著 吴石头, 王洋洋,肖益林. 2021 《稳定同位素地球化学》第8版/(德)约亨 霍夫斯(Jochen Hoefs),中国科学技术大学出版社,ISBN 978-7-312-05201-9
专利 吴石头 等. 一种原位微区磷灰石Lu-Hf定年方法 中国 ZL 2023 1 0028497.7. 授权公告日:2023.08.23 吴石头 等. 一种原位微区石榴石Lu-Hf定年方法 中国 ZL 202310045795.7. 授权公告日:2023.08.18 吴石头 等. 一种原位微区磷钇矿Lu-Hf定年方法 中国 ZL 2023 1 0028565.X. 授权公告日:2023.06.16 Shitou Wu et al. METHOD FOR SIMULTANEOUSLY MEASURING THE VALUE OF FORSTERITE AND TRACE ELEMENTS IN OLIVINE 2023 Unite States, Patient No: US 11,664,208 B2 吴石头 等. 一种原位微区方解石U-Pb定年方法 中国. ZL 2021 1 0891559.8. 授权公告日:2022.10.09 吴石头 等. 一种同时测定橄榄石中的镁橄榄石值和微量元素方法 中国. ZL 2020 1 0404435.8. 授权公告日:2021.04.09
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